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Beilstein J. Org. Chem. 2016, 12, 2005–2011, doi:10.3762/bjoc.12.187
Graphical Abstract
Scheme 1: The Sonogashira reaction.
Figure 1: Cyrene vs. DMF – selected physical properties [31,32].
Figure 2: Aldol products 4a and 4b and single crystal X-ray structure of 4b.
Scheme 2: Cyrene-based Sonogashira cross-coupling: Substrate scope. Isolated yields. aYield using DMF as solv...
Scheme 3: Cacchi-type annulation of o-amino/hydroxy iodoarenes. Isolated yields. aYield using DMF as solvent.